Abstract:The standards of pure precious metal products and the corresponding testing standards issued at home and abroad were summarized. The development history and current situation of precious metal products and their testing technical standards were reviewed. The differences of product standard parameters at home and abroad as well as the advantages and disadvantages of various testing technology methods were compared. The existing problems at present were analyzed and discussed. The development trend and hot spots in future were prospected.
方卫, 李世宇, 任传婷, 马媛, 王应进, 杨晓滔. 纯贵金属产品及其检测技术标准发展历史和现状[J]. 冶金分析, 2020, 40(4): 15-22.
FANG Wei, LI Shi-yu, REN Chuan-ting, MA Yuan, WANG Ying-jin, YANG Xiao-tao. Development history and current situation of pure precious metal products and their testing technical standards. , 2020, 40(4): 15-22.
董守安.贵金属的精密分析[J].贵金属,1994,15(1):73-78.DONG Shou-an.Precision analysis of precious metals[J].Precious Metals,1994,15(1):73-78.
[3]
董守安.贵金属的精密库仑分析-I.金纯度的测定[J].分析实验室,1991,10(5):19-22.DONG Shou-an.Precise coulometric titration of the precious metals I:Determination of gold in pure gold[J].Chinese Journal of Analysis Laboratory,1991,10(5):19-22.
[4]
方卫,杨玉芳,赵云昆,等.发射光谱法同时测定纯铂中21个杂质元素[J].贵金属,2002,23(1):36-38.FANG Wei,YANG Yu-fang,ZHAO Yun-kun,et al.Determination of 21 impurities in pure platinum by emission spectrometry method[J].Precious Metals,2002,23(1):36-38.
[5]
刘伟,方卫.原子发射光谱法测定锇中21个杂质元素[J].贵金属,2003,24(2):53-56.LIU Wei,FANG Wei.The determination of 21 impurities in osmium by AES[J].Precious Metals,2003,24(2):53-56.
[6]
ASTM.E1446-13 Standard test method for chemical analysis of refined gold by direct current plasma atomic emission spectrometry[S].American,2013.
[7]
ASTM.E378-97 Standard test method for spectrographic analysis of silver by the powder technique (Withdrawn 2004)[S].American,2004.
M P Mogorosi.The optimization and calibration of spark-optical emission spectroscopy for the analysis of trace impurities in ultra-pure Pt,Pd and Rh[D].Johannesburg:Science University of the Witwatersrand,2014.
[18]
刘伟,方卫,何姣,等.还原、沉淀分离ICP-AES测定纯银中20个杂质元素[J].贵金属,2009,30(2):53-58.LIU Wei,FANG Wei,HE Jiao,et al.Separation with reduction and precipitation for determination of 20 impurities in pure silver by ICP-AES[J].Precious Metals,2009,30(2):53-58.
[19]
李光俐,甘建壮,马媛,等.多元光谱拟合校正电感耦合等离子体原子发射光谱法测定铑粉中19种杂质元素[J].冶金分析,2014,34(5):35-40.LI Guang-li,GAN Jian-zhuang,MA Yuan,et al.Determination of nineteen impurity elements in rhodium powder by inductively coupled plasma atomic emission spectrometry multi-component spectral fitting correction[J].Metallurgical Analysis,2014,34(5):35-40.
[20]
李光俐,徐光,何姣,等.多元光谱拟合ICP-AES法同时测定铂中22个杂质元素[J].贵金属,2010,31(4):46-51.LI Guang-li,XU Guang,HE Jiao,et al.MSF for determination of 22 impurities in pure platinum by ICP-AES[J].Precious Metals,2010,31(4):46-51.
[21]
刘湘生,张安定,刘玉龙,等.电感耦合等离子体质谱法测定高纯金中痕量杂质[J].分析化学,2000,28(3):322-325.LIU Xiang-sheng,ZHANG An-ding,LIU Yu-long,et al.Determination of high purity gold by inductively coupled plasma-mass spectrometry[J].Chinese Journal of Analytical Chemistry,2000,28(3):322-325.
[22]
李光俐,何姣,周世平,等.ICP-MS法测定高纯铂中18个痕量杂质元素[J].贵金属,2015,36(3):60-65.LI Guang-li,HE Jiao,ZHOU Shi-ping,et al.Determination of 18 trace-impurities in high purity platinum by ICP-MS[J].Precious Metals,2015,36(3):60-65.
[23]
李秋莹,甘建壮,李立新,等.ICP-MS法测定高纯钯中18个痕量杂质元素[J].贵金属,2017,38(4):49-55.LI Qiu-ying,GAN Jian-zhuang,LI Li-xin,et al.Determination of 18 trace impurities in high purity palladium by ICP-MS[J].Precious Metals,2017,38(4):49-55.
[24]
詹科,孙平,种娜.辉光放电质谱仪直接测定高纯银的痕量杂质元素[J].硅谷,2014(9):126-127.ZHAN Ke,SUN Ping,ZHONG Na.Determinating of trace elements in high-purity sliver by GDMS[J].Silicon Valley,2014(9):126-127.
[25]
刘红,魏茹欣,李爱嫦,等.辉光放电质谱法测定铱及铱合金中的16种杂质[J].分析试验室,2018,37(2):188-191.LIU Hong,WEI Ru-xin,LI Ai-chang.et al.Analysis for 16 elements in iridium alloys by glow discharge mass spectrometry[J].Chinese Journal of Analysis Laboratory,2018,37(2):188-191.